From 44b8ef1057a2cae7016086e448e9f128acc63849 Mon Sep 17 00:00:00 2001 From: Matthew Rowles Date: Thu, 19 Jun 2025 22:01:33 +0800 Subject: [PATCH 1/2] example PD_CALIB_INCIDENT_INTENSITY --- cif_pow.dic | 56 ++++++++++++++++++++++++++++++++++++++++++++++++++++- 1 file changed, 55 insertions(+), 1 deletion(-) diff --git a/cif_pow.dic b/cif_pow.dic index 3399f86..9caf692 100644 --- a/cif_pow.dic +++ b/cif_pow.dic @@ -2708,7 +2708,7 @@ save_PD_CALIB_INCIDENT_INTENSITY _definition.id PD_CALIB_INCIDENT_INTENSITY _definition.scope Category _definition.class Set - _definition.update 2023-06-10 + _definition.update 2025-06-19 _description.text ; This section defines the parameters used for the incident intensity @@ -2727,6 +2727,58 @@ save_PD_CALIB_INCIDENT_INTENSITY _name.object_id PD_CALIB_INCIDENT_INTENSITY _category_key.name '_pd_calib_incident_intensity.instr_id' + loop_ + _description_example.case + _description_example.detail +; + _pd_calib_incident_intensity.instr_id a3643812 + _pd_calib_incident_intensity.incident_counts 4231 + _pd_calib_incident_intensity.special_details 'From beam monitor.' +; +; + The number of counts incident on the specimen in the instrument + identified as a3643812 is 4231, as measured by a beam monitor. The + uncertainty on the incident counts is given as the square root of the + counts. +; +; + _pd_calib_incident_intensity.instr_id 9deaa4f1 + _pd_calib_incident_intensity.incident_intensity 453.3 + _pd_calib_incident_intensity.incident_intensity_su 1.6 + _pd_calib_incident_intensity.diffractogram_id STANDARD_30ffb964 + _pd_calib_incident_intensity.phase_id SRM1796_15341c3a +; +; + In the instrument identified as 9deaa4f1, the intensity incident on the + specimen is 453.3 ± 1.6. This was determined through an analysis of + the diffractogram, STANDARD_30ffb964, which contains the phase, + SRM1796_15341c3a. +; +; + _pd_instr.id a3643812 + _pd_diffractogram.id WHITE_POWDER + + loop_ + _pd_data.point_id + _pd_meas.2theta_scan + _pd_meas.counts_total + _pd_proc.intensity_total + _pd_proc.intensity_total_su + 1 10.02 2774 0.6556 0.0160 + 2 10.04 2923 0.6909 0.0166 + 3 10.06 3096 0.7317 0.0173 + 4 10.08 3159 0.7466 0.0176 + # ... +; +; + The measured intensities for the diffractogram "WHITE_POWDER" + collected on the instrument "a3643812" have been processed to + give the normalised intensity at each point in the scan using + the incident intensity calibration linked to that instrument. + The SU values have also been calculated for the + _pd_proc.intensity_total values. +; + save_ save_pd_calib_incident_intensity.diffractogram_id @@ -12830,4 +12882,6 @@ save_ Updated descriptions of data items linked to _pd_data.point_id to clarify that identical values refer to the same data point in each disparate loop; they cannot be assigned values independently. + + Added example to PD_CALIB_INCIDENT_INTENSITY ; From db4ec7e615b39218c907541634bfeef7aa6d76a9 Mon Sep 17 00:00:00 2001 From: Matthew Rowles Date: Thu, 19 Jun 2025 23:26:51 +0800 Subject: [PATCH 2/2] tabs removed --- cif_pow.dic | 8 ++++---- 1 file changed, 4 insertions(+), 4 deletions(-) diff --git a/cif_pow.dic b/cif_pow.dic index 9caf692..41b79f4 100644 --- a/cif_pow.dic +++ b/cif_pow.dic @@ -2764,10 +2764,10 @@ save_PD_CALIB_INCIDENT_INTENSITY _pd_meas.counts_total _pd_proc.intensity_total _pd_proc.intensity_total_su - 1 10.02 2774 0.6556 0.0160 - 2 10.04 2923 0.6909 0.0166 - 3 10.06 3096 0.7317 0.0173 - 4 10.08 3159 0.7466 0.0176 + 1 10.02 2774 0.6556 0.0160 + 2 10.04 2923 0.6909 0.0166 + 3 10.06 3096 0.7317 0.0173 + 4 10.08 3159 0.7466 0.0176 # ... ; ;