diff --git a/cif_pow.dic b/cif_pow.dic index bf5baaa..806b2b9 100644 --- a/cif_pow.dic +++ b/cif_pow.dic @@ -12316,6 +12316,37 @@ save_PD_SPEC _name.category_id PD_GROUP _name.object_id PD_SPEC _category_key.name '_pd_spec.id' + _description_example.case +; + _pd_spec.prep_id ABC123_main + _pd_spec.id ABC123_03 + _pd_spec.description 'Iron ore from FeOre Inc. ID number ABC123' + _pd_spec.mount_mode reflection + _pd_spec.mounting 'back-packed powder pellet' + _pd_spec.orientation horizontal + _pd_spec.preparation + ; + 50 g of received sample was homogenised and cone-and-quartered + to obtain a 3 g split. 1 g of ɑ-alumina was added as an internal + standard. The specimen was micronised for 15 min with 15 ml of + ethanol and dried at 45 °C. The resulting powder was backpressed + into a holder with a semi-automated press. + ; + _pd_spec.shape flat_sheet + _pd_spec.size_axial 25.0 + _pd_spec.size_equat 25.0 + _pd_spec.size_thick 3.5 +; + _description_example.detail +; + A specimen of iron ore, from FeOre Inc., with an added internal + standard was prepared for analysis. The sample from which the specimen + was prepared is identified by a _pd_prep.id value of "ABC123_main". + The data were collected in reflection on an instrument where the + incident and diffracted beams are vertical. The specimen flat, and is + 25.0 x 25.0 mm, or it could be inferred to be 25 mm diameter. + The specimen was prepared as described. +; save_ @@ -13008,5 +13039,5 @@ save_ disparate loop; they cannot be assigned values independently. Added examples to PD_CALC_OVERALL, PD_CALIB_INCIDENT_INTENSITY, PD_CHAR, - _pd_diffractogram.id, PD_PHASE_MASS, PD_PROC_LS. + _pd_diffractogram.id, PD_PHASE_MASS, PD_PROC_LS, PD_SPEC. ;